多功能液體/固體表面張力測試儀Tensίίo

新世代多功能液體/固體表面張力測試儀 -Tensίίo


傳統力學及影像分析的結合”–傳統理論+科技創新

頂級張力儀需要的不僅僅是一個精確的力學感測器和最大動態範圍的精密定位系統,還需要改變視角關注使用者和使用者的任務需求。Tensíío新世代多功能液體/固體表面張力測試儀- 可以使您的實驗室工作更方便、更靈活、更省時同時含括更大範圍的使用者應用需求


理論上,張力儀的結構很簡單:在測力裝置下方加一個可移動的樣品台。但是開發一款一流的張力儀是截然不同的,開發一款一流的張力儀需要的不僅僅是一個精確的力學傳感器(我們做到了)和定位系統的大動態範圍(我們開發了),還需要改變視角,關注用戶和他們的任務——您和您的任務。這款儀器可以使您的實驗室工作更方便、靈活和省時。我們認為,Tensíío就是這樣的儀器。


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l液體表面張力測量

l固體接觸角、表面自由能測量

l粉體接觸角、表面自由能測量

l界面活性劑CMC的評估

l液體密度+固體密度測量分析

l沉降速率+侵透測試

l-相間黏著性評估分析

l影像分析接觸角+面積+輪廓偵測


INSTRUMENT DIMENSIONS

Footprint290 mm × 360 mm (W × D)
Height560 mm
Weight (without accessories)29 kg

TEMPERATURE MEASUREMENT

Range of temperature measurement-60 to 450 °C
Resolution0.01 °C
Precision0.05 °C
Accuracy0.5 °C
Internal sensorsample stage
External sensoroptional: sample vessel

POWER SUPPLY

Voltage100 to 240 V
Power consumption40 W
Frequency47 to 63 Hz

ENVIRONMENT

Operating temperature15 to 30 °C
Humidity> 30% without condensation

TEMPERATURE CONTROL

Type of temperature controlliquid (-10 to 130 °C)
electrical (50 to 300 °C)
Peltier (-15 to 135 °C)
Range of temperature control-15 to 300 °C

INTERFACES

PCUSB 3.0
AuxiliaryCAN / CANopen
Thermostatoptional
(quick lock fittings)
Inert gasoptional

HOUSING AND PERIPHERALS

Built-in bubble leveloptional (electronic bubble level)
Built-in and software-controlled ionizeroptional
Glass windshield doorsyes
Stainless steel measuring compartmentyes
Touch displayintegrated color IPS display
(1024 x 600 pixel, size 7'')

SAMPLE STAGE

Travel distance120 mm
Simple platformoptional
Temperature control jacketoptional: 50 mm, 70 mm
Inverse CMCoptional: cone-shaped vessel
Integrated sample stageyes

DRIVE

Resolution16 nm
Travel speed0.001 to 800 mm/min
Type of motorbrushless DC servo motor

CAMERA SYSTEM (STANDARD)

ConnectionUSB 3.0
Performance15 fps at 2560 × 1920 px

OPTICS (STANDARD)

Focusfixed
Zoom1.4× zoom, fixed
Field of view6 mm × 4.5 mm
Resolution of optics2.3 µm

OPTICAL HEIGHT SENSOR

Resolution0.05 µm

FORCE MEASUREMENT

Maximum load210 g
Resolution10 µg
Measurement rate50 Hz
Adjustmentfully automated
internal weigth
Locking mechanismautomatic

SOFTWARE

Software typeADVANCE
Available software modulessurface tension (SFT) / interfacial tension (IFT)
contact angle (CA) / surface free energy (SFE)
critical micelle concentration (CMC)
liquid density
solid density
special purpose
adhesion analysis
sedimentation / penetration

SURFACE FREE ENERGY OF SOLIDS

Resultssurface free energy (SFE)
Modelsequation of state
Zisman
Fowkes
Wu
Owens-Wendt-Rabel-Kaelble
extended Fowkes
acid-base theory

WASHBURN

Resultscontact angle (CA)
Resolution0.01°
Range0 to 90°
Typeadvancing

WILHELMY CONTACT ANGLE

Minimum fiber diameter20 µm
Resultscontact angle (CA)
Range0 to 180°
Resolution0.01°
Typeadvancing
receding

WILHELMY PLATE

Resultssurface tension (SFT)
interfacial tension (IFT)
critical micelle concentration (CMC)
Range1 to 2000 mN/m
Resolution0.002 mN/m

DU NOÜY RING

Resultssurface tension (SFT)
interfacial tension (IFT)
critical micelle concentration (CMC)
Range1 to 2000 mN/m
Resolution0.001 mN/m
Correction methodHarkins-Jordan
Huh-Mason
Zuidema-Waters
linear correction
no correction

LIQUID DENSITY

Liquid density range1 to 2200 kg/m³
Resolution0.1 kg/m³
Precision3 kg/m³

SOLID DENSITY

Solid density range1000 to 20000 kg/m³
Resolution1 kg/m³
Precision±3 kg/m³

PENETRATION

Resultsgraph: mass vs. time

ROD

Resultssurface tension (SFT)
interfacial tension (IFT)
critical micelle concentration (CMC)
Range1 to 2000 mN/m
Resolution0.02 mN/m

SEDIMENTATION

Resultsgraph: mass vs. time

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CP503

The CP0503 set includes an E2 reference weight with a mass of 100 g with which the force sensor of your K11 or K100C Force Tensiometer can be reliably adjusted. The actual value for the mass measured by the force sensor is adjusted to the nominal value of the accurate reference weight. The attached certificate from the German Calibration Service (DKD) indicates the high level of precision of the weight. The set also includes a hook and force sensor adapter to facilitate easy attachment of the weight and a pair of tweezers to ensure the weight can be attached without soiling. A high-quality case is provided for safe storage of the set.


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CP14

Calibration set for the force sensor

 

The CP14 calibration set is available for regular calibration of your tensiometer. The set includes three E2 standard weights (0.2 g; 0.5 g; 1.0 g), which are certified in compliance with OIML R111. The provided certificate from the German Calibration Service (DKD) indicates the high level of precision of the weight.

A weighing pan on which the weights can be easily placed and a pair of tweezers to ensure the weight can be applied without soiling are also included in the set. A high-quality case is provided for safe storage of the weights.


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PA0910

Wind shield hood

 

Strong air streams can have a negative impact on the high-precision force sensor of your tensiometer even when the measurement chamber is closed. The complete measuring instrument fits under the PA0910 wind shield hood, which can be used in order to optimize the measurement of setups under a lab hood, for example.



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DE0601

The DE0601 set enables accurate determination of the density of Newtonian liquids using the buoyancy force on an immersion body (Archimedes’ principle). The materials – silicon crystal for the immersion body and platinum-iridium for the accompanying holder – are inert and can be used for virtually all liquids with a maximum density of 2.3 g/cm3. A high-quality protective box is provided for safe storage of the set.



 

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DS0810

Automatic dosing with one Micro Dispenser for CMC measurements

 

Our specially developed Micro Dispensers equip the K100 for measuring the critical micelle concentration (CMC) with the utmost precision, using one or two Dispenser units (DS0810 or DS0820). The surfactant concentration range is set up and measured fully automatically.



   
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DS0820

Automatic dosing with two Micro Dispensers for CMC measurements

 

Our specially developed Micro Dispensers equip the K100 for measuring the critical micelle concentration (CMC) with the utmost precision, using one or two Dispenser units (DS0810 or DS0820). The surfactant concentration range is set up and measured fully automatically.

 

Working with two Micro Dispensers, where one dispenses the liquid and the other extracts the same volume, has great advantages. This enables a very wide concentration range with a high density of measuring points to be created in order to measure the CMC with high accuracy. Wrong measurements due to a too highly concentrated parent solution are virtually ruled out, as it can be diluted by several orders of magnitude and the CMC measured with high probability.


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PL01

Standard measuring probe for the Wilhelmy plate method

 

The PL01 is our proven plate geometry for measuring the surface and interfacial tension using the Wilhelmy plate method. The dimensions of the plate comply exactly with the form specified in international standards and thus enable a high level of repeatability for the analyses. As the plate is made of the precious metal platinum it has an extremely high surface free energy and therefore also the required excellent wetting properties. These are further optimized by its homogenously roughened surface.

 

A simple clamping mechanism allows especially fast insertion of the plate. Its safe storage is assured through a high-quality protective box provided.

 

A PLC01 version of the plate with a certificate from an independent testing institute is also available.



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PL02

Wilhelmy plate measuring probe for small sample volumes

 

The PL02 measuring probe enables measurement of the surface tension with the Wilhelmy plate method in the case of small sample volumes. It is the same size (wetted length) as our standard PL01 plate and is also ideally wettable being made from the same precious metal platinum, but it is rolled cylindrically so it only requires a small surface area of the liquid. A high-quality protective box is provided for safe storage of the plate.

The scope of delivery of the rolled plate also includes a measuring vessel that can be used flexibly for different sample volumes: The hollow has a capacity of 5 mL and the vessel has concentric rings on its underside that can be filled with up to 1.2 mL or up to 0.2 mL.


 

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PL03

Rod-shaped probe for measurements with the Wilhelmy method

 

The rod-shaped probe PL03 can be used as an alternative to the rolled PL02 for measuring the surface tension using the Wilhelmy method with small sample volumes. Thanks to its small diameter it is possible to carry out measurements in small vessels, but unlike the PL02 it also enables measurement of the interfacial tension. The rod is made of the ideally wettable precious metal platinum. A high-quality protective box is provided for its safe storage.

The scope of delivery of the rod also includes a measuring vessel that can be used flexibly for different sample volumes. The hollow has a capacity of 5 mL and the vessel has concentric rings on its underside that can be filled with up to 1.2 mL or up to 0.2 mL.



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RI01

Standard measuring probe for the Du Noüy ring method

 

The RI01 ring is our high-precision standard measuring probe for surface and interfacial tension using the Du Noüy ring method. The wire ring made of a platinum-iridium precious metal alloy is ideally wettable; the hardness of the iridium makes the measuring probe especially robust. The ring geometry is only connected to the shaft at two junctures, so that any disturbing influences on wetting are negligible.

A simple clamping mechanism allows especially fast insertion of the ring. Its safe storage is assured through a high-quality protective box provided.

An RIC01 version of the ring with a certificate from an independent testing institute is also available.



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RI02

Du Noüy ring measuring probe for small sample volumes

 

The special measuring probe RI02 is used for measuring the surface tension with the ring method where only small sample volumes are available. Measurements with volumes as of 1 mL are possible thanks to the reduced diameter of the ring.

Like the standard RI01 ring, the RI02 is also made of a platinum-iridium alloy so its combines ideal wettability with the necessary metal hardness. Its design with only two contact points between the ring and the shaft and its shape accuracy ensure a high level of precision. A special vessel for small sample volumes is included in the scope of delivery as well as a high-quality protective box in which it can be safely stored.


 

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SH0601

Sample holder for contact angle measurements on plate-shaped samples

 

The SH0601 sample holder enables tensiometric measurements of the contact angle of plate-shaped solids using the Wilhelmy method. The sample holder is inserted into the tensiometer force sensor adapter in one quick step.

The clip of the holder presses the sample against the pressing surface arranged exactly horizontally to the shaft, so that the sample is immersed in an exact vertical position during measurement. Whereby the sample is positioned on the horizontal upper edge of the pressing surface and thus straightly aligned.

 



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SH0602

Sample holder for contact angle measurements on foils and films

   

In order to carry out tensiometric measurements of the contact angle on foil and film samples using the Wilhelmy method, these samples are fixed firmly with the SH0602 special sample holder. The wide pressing surface of the clip that is arranged level with the shaft ensures the sample is firmly fixed and simplifies straight and vertical positioning of the sample during immersion in the test liquid.


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SH0620

Sample holder for contact angle measurements on packed or bundled fibers

 

We have developed the SH0620 sample holder for measuring the contact angle on packed or bundled fibers using the Washburn method. The aluminum tube is quickly and simply equipped with a filter paper base and filled with the fiber samples. The accurate force sensor of the tensiometer measures the increase in mass with respect to time during adsorption to the fibers and the contact angle is calculated from the result.

The matching filter paper SH0621 is available from us in sets of 100 filters.

 



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SH0640

Measuring probe for analyzing the sedimentation behavior of dispersions

 

The SH0640 measuring probe enables the analysis of the sedimentation speed of particles in a dispersion. After thorough mixing with the integrated stirrer of the Force Tensiometer – K100, the particles sink into the inverted hollow cone of the measuring probe. The force sensor of the instrument measures the increase in mass accurately and time-dependently.

 



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SH0650

Measuring probe for analyzing the penetration resistance of sediments

 

The SH0650 measuring probe is used to analyze the penetration resistance of a sediment against a solid mass. This involves the software-controlled movement of the sediment upwards against the solid stainless steel cone of the measuring probe. The force sensor of the Force Tensiometer – K100 registers the sediment resistance that opposes the weight force. The measurement curve provides information about the density and solidity of the sediment.

 

 

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SH0801

Sample holder for contact angle measurements on single fibers

 

The SH0801 fiber holder makes preparation of single fiber contact angle measurements using the Wilhelmy method simple and reliable. The fiber is fixed to the reception surface of the stainless steel holder with the aid of double-sided adhesive foils.

 

The matching SH0802 adhesive foils are available from us in sets of 50 foils.

 



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SH0810

Washburn sample holder

 

The SH0810 sample holder enables measurements of the contact angle on powders and pigments using the Washburn method. The glass sample tube can be equipped with a filter paper base using a clamping ring quickly and simply and then filled with the sample. It is easy to check the height and evenness of the filling in the transparent tube. The sample holder is attached to the SH0812 force sensor adapter, which must be ordered separately, in a matter of seconds.

One set of matching filter paper is included and also available from us in sets of 100 filters with the designation SH0621. Spare glass tubes with the designation SH0822 can also be ordered.



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SH0812

Sample holder adapter for Washburn measurements

 

The sample holder adapter SH0812 is required to attach the Washburn sample holder SH0810 or measuring cell SH0820 to the force sensor of your tensiometer. The clamp of the adapter keeps the sample holder or cell safely in position.



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SH0820

Washburn sorption cell for optimized sample preparation

 

The SH0820 Washburn sorption cell for contact angle measurements on powders and pigments is made of stainless steel and specially designed for maximum reproducibility of sample preparation. The bottom of the cell is fitted with a filter paper, followed by the insertion of the provided sorption glass tube. Finally, a cap is screwed onto the cell and presses the tube against the cell's bottom, keeping the paper filter absolutely fixed. With this method, the pressure on the filter from below when immersing the powder-filled tube cannot influence the measurement. Powder wetting analysis can be even more accurate when combining the SH0820 Washburn sorption cell with our separately available preparation set SH0824.    

The SH0812 force sensor adapter is additionally required for using the sorption cell SH0820. One set of matching filter paper is included and also available from us in sets of 100 filters with the designation SH0823. Spare glass tubes with the designation SH0822 can also be ordered.





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SH0824

Preparation set for Washburn sorption measurements

 

Our preparation set SH0824 is a helpful tool for preparing the Washburn sorption tube and packing the powder sample reproducibly, which is important for obtaining reliable contact angle results. The set consists of a fitted shape for inserting the powder-filled Washburn cell SH0820 and a plunger for compressing the sample.

 

The shape has a slightly dished base so the filter base is pressed into the dish and curves in a reproducible manner. In this way, air bubbles, which could influence the measurement, do not adhere on immersion.

 

The plunger compresses the powder reproducibly without bodily force and only as a result of its inherent weight. The mass can be flexibly matched to the particular sample characteristics, as with a dumbbell, by fitting up to four discs, each weighing 500 g.



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SV01

PTFE sample vessels in different sizes

 

Our sample vessels SV21/SV11/SV01 made of PFTE are used if glass is not suitable as a sample vessel material. Due to the fact that their surfaces are difficult to wet, the PTFE vessels are easy to clean and therefore well suited for liquids that cause severe soiling such as inks, varnishes or adhesives. The PTFE vessels also optimize the analysis of surfactants that adsorb strongly on glass.

  • SV01: special sample vessel for the smallest sample volumes. The SV01 is included in orders for a RI02/RI0902, PL02/PL0902 or PL03/PL0903 special probe, but can also be ordered separately.

 

We offer matching adapters for the SV11 and SV01 for positioning the sample vessel centrally in the thermostat jacket of the tensiometer.

 

 

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SV10

Glass sample vessels with different sizes

 

The SV30/SV20/SV10 fire-proof glass sample vessels are the standard vessels for analyses carried out with our tensiometers. Easy to clean and resistant to most chemicals, they are suitable for virtually all test liquids. The vessels come in different sizes to optimize the measurement of different sample volumes.

SV10: set of 6 sample vessels with an outer diameter of 50 mm for medium sample volumes

 

 

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SV11

PTFE sample vessels in different sizes

 

Our sample vessels SV21/SV11/SV01 made of PFTE are used if glass is not suitable as a sample vessel material. Due to the fact that their surfaces are difficult to wet, the PTFE vessels are easy to clean and therefore well suited for liquids that cause severe soiling such as inks, varnishes or adhesives. The PTFE vessels also optimize the analysis of surfactants that adsorb strongly on glass.

  • SV11: vessels with an outer diameter of 50 mm for medium sample volumes

  • We offer matching adapters for the SV11 and SV01 for positioning the sample vessel centrally in the thermostat jacket of the tensiometer.

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    SV12

    Cover plates for sample vessels during measurement

 

During measurement the SV26/SV12 cover plates ensure reduced heat exchange with the surroundings as well as constant measuring temperatures with temperature-controlled samples. In addition, the cover plates reduce evaporation of the sample, which in turn optimizes the accuracy of the analysis in the case of long-term measurements and volatile substances.

 
  • SV12: for sample vessels with a diameter of 50 mm

 

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SV13

Disposable aluminum sample vessel

 

Liquids that cause severe soiling or that cure can be analyzed trouble-free with the aid of the SV13 disposable sample vessel. The vessel has an outer diameter of 50 mm and can hold 20 mL of a sample. The SV13 is available in sets of 100 vessels.

 

We also offer a matching adapter that positions the sample vessel centrally in the thermostat jacket and ensures optimum temperature control.

 

 

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SV20

Glass sample vessels with different sizes

 

The SV30/SV20/SV10 fire-proof glass sample vessels are the standard vessels for analyses carried out with our tensiometers. Easy to clean and resistant to most chemicals, they are suitable for virtually all test liquids. The vessels come in different sizes to optimize the measurement of different sample volumes.

  • SV20: set of 6 standard vessels with an outer diameter of 70 mm, that are an exact fit for the standard thermostat jacket of our tensiometers

 

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SV21

PTFE sample vessels in different sizes

 

Our sample vessels SV21/SV11/SV01 made of PFTE are used if glass is not suitable as a sample vessel material. Due to the fact that their surfaces are difficult to wet, the PTFE vessels are easy to clean and therefore well suited for liquids that cause severe soiling such as inks, varnishes or adhesives. The PTFE vessels also optimize the analysis of surfactants that adsorb strongly on glass.

  • SV21: vessels with an outer diameter of 70 mm, that are an exact fit for the thermostat jacket of our tensiometers

 

 

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SV26

Cover plates for sample vessels during measurement

 

During measurement the SV26/SV12 cover plates ensure reduced heat exchange with the surroundings as well as constant measuring temperatures with temperature-controlled samples. In addition, the cover plates reduce evaporation of the sample, which in turn optimizes the accuracy of the analysis in the case of long-term measurements and volatile substances.

  • SV26: for sample vessels with a diameter of 70 mm

 

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SV30

Glass sample vessels with different sizes

 

The SV30/SV20/SV10 fire-proof glass sample vessels are the standard vessels for analyses carried out with our tensiometers. Easy to clean and resistant to most chemicals, they are suitable for virtually all test liquids. The vessels come in different sizes to optimize the measurement of different sample volumes.

  • SV30: set of 6 sample vessels with an outer diameter of 98 mm (temperature-controlled measurements are possible with the special TJ34 thermostat jacket)

 

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TJ22

Thermostat jacket adapters for small sample vessels

 

The thermostat jacket of our tensiometers is designed for standard sample vessels with a diameter of 70 mm. The TJ22, TJ23 and TJ24 adapters are available for various smaller sample vessels. The adapters are made of the good heat-conductive metal aluminum, thus ensuring even temperature control of the sample. The adapters also make it easier to position the sample vessel in the center of the measuring instrument.

  • TJ22: adapter for the SV10 sample vessel (50 mm outer diameter)

 

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TJ23

Thermostat jacket adapters for small sample vessels

 

The thermostat jacket of our tensiometers is designed for standard sample vessels with a diameter of 70 mm. The TJ22, TJ23 and TJ24 adapters are available for various smaller sample vessels. The adapters are made of the good heat-conductive metal aluminum, thus ensuring even temperature control of the sample. The adapters also make it easier to position the sample vessel in the center of the measuring instrument.

  • TJ23: adapter for the SV01 sample vessel for small sample volumes

 

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TJ24

Thermostat jacket adapters for small sample vessels

 

The thermostat jacket of our tensiometers is designed for standard sample vessels with a diameter of 70 mm. The TJ22, TJ23 and TJ24 adapters are available for various smaller sample vessels. The adapters are made of the good heat-conductive metal aluminum, thus ensuring even temperature control of the sample. The adapters also make it easier to position the sample vessel in the center of the measuring instrument.

  • TJ24: adapter for the SV13 disposable sample vessel

 

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TJ25

Inert-gas hood

 

We have developed the TJ25 inert-gas hood to enable measurements of oxygen-sensitive substances. The TJ25 is equipped with a connection for inert gas and is attached to the thermostat jacket of the tensiometer in a few quick steps. The two-part hood ensures the lowest possible gas exchange with the surroundings.

 

 

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TJ40

Thermostat jacket with stirring function

 

The TJ40/TJ41 thermostat jacket equips your tensiometer for temperature-controlled measurements of between -10 and 130 °C. The jacket has quick-locks for fast connection to a flow-thorough thermostat and is made of the excellent heat conductor brass. An integrated temperature sensor ensures continuous communication of the temperature inside the jacket. The stirrer of this accessory is regulated via ADVANCE software or the control pad of the measuring instrument and enables quick mixing of solutions and dispersions.

  • TJ40 is equipped with an induction-based magnetic stirrer so that a magnetic field is only present when stirring.


 

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TO01

Tool for adjusting distorted ring measuring probes

 

The delicate measuring probe for the Du Noüy ring method is easily bent if dropped or accidentally knocked rendering it unsuitable for the measurement. Our special TO01 tool can be used to restore the exact shape of the measuring element.

Alternatively our technical support also provides the re-alignment of deformed rings as a service or carries this out as part of the servicing of your instrument.

 

 

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TO0810

Preparation set and holder for measurement of multiple fibers

 

The thinner your fibers, the lower the measurable wetting forces. With the TO0810 fiber holder and preparation set, you can measure with up to five fibers at the same time and thus obtain even more reliable measured values thanks to five times the force.

 

The fiber holders in the set are plastic clips that fix the samples vertically using a light-curing adhesive. The clips are then precisely inserted into the five-fold adapter for the tensiometer's force sensor.

 

With the very fine tip of the supplied adhesive cartridge, the tiny drop of adhesive can be precisely dispensed. For easier handling, the cartridge sits in a holder equipped with a blue light source on the opposite side. The adhesive is cured after just 10 seconds.

 

The following components are included in the scope of supply:

 

  •  Force sensor adapter for up to five fiber samples

  • 1000 plastic clips (available as spare part SH0902)

  • Tube of adhesive, inserted in a holder with a fitted blue light source (available as spare part TO0911)

  • Scalpel with five blades

  • Scissors

  • Tweezers

 

 

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TO0910

Enhanced single fiber holder and preparation set

 

Our fiber holder and preparation set TO0910 simplifies the attachment and alignment of single fibers for precise contact angle measurements. The fiber holders in the set are plastic clips which fix the samples with the help of a UV-curing adhesive. At the same time, two V-shaped notches hold the fiber vertically. The clip is then quickly and accurately inserted in a special adapter for the tensiometer’s force sensor.

 

The adhesive cartridge supplied has a very fine tip which enables the tiny amount required to be accurately applied. For easy handling, the cartridge rests in a holder which is fitted on the opposite side with a UV light source. The adhesive cures in only 10 seconds and the measurement can begin.
The following components are included in the scope of supply:

 

  • Force sensor adapter

  • 1000 plastic clips (available as spare parts SH0902)

  • Tube of adhesive, inserted in a holder with a fitted UV light source (available as spare parts TO0911)

  • Scalpel with five blades

  • Scissors

  • Tweezers